Authors : Mohammad Tawkir Sheikh and Sushil B. Kapoor
Page Nos : 121-127
Description :
Glibenclamide (5-Chloro-N-(4-{N-(Cyclohexyl Carbonyl) Sulfamoyl]Phenethyl)-2-methoxybenzamide was used to synthesize Cu(II), Zn(II), Mo(II), Fe(II) complexes. Metal complxes were characterized by elemental analysis, IR, TGA. The crystal structure of complexes were further determined by X-ray diffraction method. The XRD data was used to calculate various parameters like crystal system, volume,density,porosity,particlesizeetc.which shows that the complexes of Cu(II) and Zn(II) are tetragonal while the complexes ofMo(II)and Fe(II) shows octahedral structure.
Key words:Glibenclamide, Crystal structure, Cu(II), Zn(II), Mo(II), Fe(II) complex.
